My problem boils down to lack of "strategy" or "analytical procedure", and maybe someone here could offer some advice.
Does anyone know of any books or other literature that could help me? I did find an article called "Hints on Phase Identification Using Powder X-ray Diffraction", which certainly raised a lot of potential problems and procedures, but which did not necessarily solve these problems or explain why the procedures would help. I am not able to find good literature on this subject. I lack criteria needed to accept a phase as present, and discard other phases as not present. Then another 20 phases share the highest score minus 1. Should I focus just on the major peaks? Are the minor ones important too? When I do a search-match analysis, I get 400 suggested phases, where 20 phases share the highest score. Then I do a peak search, and 50 peaks are detected. Too high? Too low? Does this strongly affect the phase identification?
#CRYSTALDIFFRACT SAVE HOW TO#
I know how to determine the background, but I am not sure when the background is appropriately determined. Grasping the software is not what I am concerned about. The goal: which manganese phases are present, and which dominate? Sample: respirable fraction aerosol samples from ferro- and silica manganese plants.
Instrument: PANalytical X'Pert$^3$ Powder Here follows some basic information about the experiment: I am having some trouble with qualitative phase identification using x-ray diffraction (XRD).
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